Category Archives: Materials and Equipment

Typically, scientists and researchers are the ones who have been trying to find ways to educate the public about nanotechnology (see “Public views nanotech research on TV,” SmallTimes, July/August 2007, page 4), but now artists are getting into the act.

Cris Orfescu, an artist who was born in Bucharest, Romania, is attempting to bring nanotechnology to the fore through his paintings and prints. As explained on his Website (www.cris orfescu.com), “My art is a reflection of the technological movement. I consider NanoArt to be a more-appealing and more-effective way to communicate with the general public and to raise the awareness for nanotechnology and its impact on our lives.


This nanosculpture, called Black Eye NanoOctupus (Orfescu, 2007), is priced at approximately $12,900.
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“I bring the small world in front of my audience through high-resolution electron microscope scans of natural micro- or nanostructures and nanosculptures I create by physical and/or chemical processing. I paint and manipulate digitally the monochromatic electron images and print them on canvas or fine art paper with archival inks specially formulated to last for a long time.”

Orfescu’s works were recently showcased at the Galeria Espacio Kubiko (www.galeriaespaciokubiko.com/pages/index.php) in Madrid, Spain. He has also exhibited in Paris, France; Finland; and Los Angeles, Calif. His works can command prices to $40,000.

– Marcy Koff

Chemist Margaret Blohm and her team at General Electric cheered in February 2003 when GE Plastics sold its first commercial batch of Lexan SLX, which was a major improvement over the plastic material that had been developed 50 years earlier for use on auto body surfaces. But despite warnings from colleagues that moving from plastics to nanotechnology research could be a career killer, by the time of the Lexan sale she had campaigned successfully for a job at GE Global Research as advanced technology leader on the company’s new nanotechnology program.

Today, Blohm heads a multidisciplinary team of about 100 scientists and engineers-three times the number of people she started with in 2001. The teams have announced a growing list of breakthroughs in the field of nanotechnology, including chemical and biological sensing, carbon nanotube diodes, biomimicry (butterfly wings and lotus leaves), diagnostic imaging, and ceramics. Blohm, 47, explained to Small Times’ Jo McIntyre how much she enjoys working at an international company that produces an astonishing number of products and employs nearly 320,000 people.

Q: What was the key influence in your life that led you to this position?

My mom was a chemist in 1945. Seeing her when she was in her tiny chemistry lab in a small university in Kansas is a huge part of why I’m here. I like challenges. Figuring out how to make nanotechnology work for GE was an opportunity I couldn’t pass up.

Q: How did you get started at GE?

I started in chemistry at GE Plastics, mostly. We developed resins for weatherability and flammability that got commercialized. Then I took the nanotechnology job.

Q: You spearheaded a project that led to commercializing a new material. Is that experience the reason they picked you for the nano job?

Yes, that’s part of it, I’m sure. Being part of a large multidisciplinary team was good experience. Also, I really wanted the nano job. It was more of a risk at the time: It was a whole new concept. The big question for nano was: “So, what are you going to do with it?”

Nanotechnology is a ‘how,’ not a ‘what.’ That is not an obvious career growth opportunity, but I thought it was too exciting to miss. Here was a chance to lead a nanotechnology project at a large corporation like GE. It doesn’t get any better than that. And I have the chance to do research across all of GE’s different businesses.

Q: What does working at this large corporation mean for you as a researcher?

We have the infrastructure and expertise to evaluate what nano can bring. We can “down select” (drop the project) if it seems to be getting away from a useful direction. You can get lost in a problem, it’s so cool; that keeps me up at night. But I get lots of critical feedback working with engineers.

Q: Is that what you like best about this work?

Yes. There’s also the challenge of finding products that will work at GE and the potential of finding a disruptive technology. And I enjoy working with different groups of people; disruptive nanotechnology is multidisciplinary. I used to think multidisciplinary activity was a chemist and a chemical engineer working together. Now, you have all kinds of researchers working on teams together. I tell myself I’m on a learning cliff, not a curve. And it’s every day. It’s humbling at times.

Q: What is the most important nano-based development you’ve been involved in, so far, on the nano side?

There’s one that has been really rewarding and exciting: Using nanotechnology for diagnostic imaging. There is a physicist, a chemist, and a biologist on my team. I felt we needed that mix. Earlier, we didn’t have any biology. I felt it was important to add that.

They came up with this idea of looking at magnetic particles to enhance our MRI imaging business. We did a lot of benchmarking and looked at the literature. We found an area where our strengths fit in, to be able to target different diseases.

It’s really easy to get up in the morning to come in to a project like that. That team now has 25 researchers. Medical diagnostics people are helping us evaluate it. It’s a technically challenging project with a long time line that requires FDA approvals and other requirements. There is still a long way ahead of us, but it is very rewarding.

Q: What are some other interesting ideas your teams are working on? Or do you solve problems that are brought to you?

We look at nanotechnology as an enabling technology. You need to be able to develop the tool kit, develop the materials, leverage them and, finally, bring them into products.

If we really understand how to solve these problems, we will have many applications in front of us for many different products. In 2007, we are focusing on different application areas. We started off with a more materials focus, but now we have evolved more to an application one.

Q: Would those materials include ceramics?

Yes. We’re looking at ceramics, metals, coatings, and nanotubes-materials to enable new products. We’re doing a wide range of research in structural materials and porous materials for sensors and the like. There’s a lot of catalysis [modification of the rate of a chemical reaction, usually an acceleration, by adding a substance not consumed during the reaction], with properties where you want to take advantage of the large surface area of nanoparticles. But particles can be very dense, because they are so small.

So, the question becomes: “How do you get the advantages of the positive features without getting trapped in the negative?” Then, you can use it for nanotechnology applications and not suffer loss of materials and flow. That gets you into a lot of uses, such as catalysis and sensing. You can put nanoparticles into a very hot part of a process and still be able to sense and detect low levels of gases like carbon dioxide. You can get gas flow-through, but can also use it with gas separation membranes where you want to get high sensitivity and selectivity.

Q: Do you have any commercially successful nano developments thus far?

My group was given the target for the longer-term, higher-risk areas. We don’t work on the shorter-term solutions, such as improving existing products, so we don’t have anything directly commercial coming out of my program.

At Global Research we already have a whole selection of products to work with. I talk to the different divisions within GE all the time: energy, health care, and aviation. I have to work closely with all of them to make sure we’re on the right path. You get a sense of the broad spectrum across many disciplines and you can use developments across the product line.

The other spectrum is me. My job is to evaluate projects as quickly as I can and move things down the pipeline. There’s a couple of things we have that I can’t talk about right now, but we are now starting to get products into the business. The smaller ones are ones you can implement faster. The really exciting ones, where we’re looking at things differently, take longer to get there. That’s what my charter was: to go after the big ones and figure out what they are.

Q: What barriers do you see to commercialization within a large company?

Barriers are technical and financial. I have a bias working at GE. We have a 100-year history of driving research to the market. I think a company like GE is perfectly positioned to really win with nanotechnology. To really win takes time. That’s a big worry of mine-managing expectations. The payoff will be huge.

Again, I think finding the fit (a lot of the world is doing this, asking where’s the real fit with this cool idea?) is key. To have the diversity of products across GE to look at is a chance of a lifetime.

Q: What challenges do you face in managing nanotechnology research programs and scientists?

The challenge of dealing with a lot of enthusiasm and making sure we stay on track with business impact and not just really cool technology. It can be hard on folks who have a good idea that’s not ready for a specific business use. An even bigger challenge is doing matrix managing. I’ve never been a fan, but I love it now. Matrix managing is the process of influencing organizations or departments or other structures where you don’t have individuals directly reporting to you, to help them recognize the mutual benefit of what they are working on.

I matrix manage the people on the various research teams. I reach in to their team and work with them. For example, a chemist is on one team and can join my team as well. It’s usually a management nightmare, but it has worked here. It’s communication both ways. They aren’t isolated from business challenges and opportunities. Matrixing helps do that.

That keeps me well tapped in and we get to know what’s working and what’s not. But also they get to see what’s working and this helps the information flow in all ways.

Q: What would you like to see in the future for nanotechnology?

I want nanotechnology to be so pervasive it’s not a new thing.


The Blohm File

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Schenectady, N.Y.-born Margaret M. Blohm received her PhD in inorganic chemistry from the University of Minnesota in 1985. She holds more than 10 U.S. patents, with a specialty in the chemistry of polymers. She joined GE Global Research in Niskayuna, N.Y., in 1987. In 1997, she was named Lab Manager of the Weatherables and Special Effects Laboratory, where she worked on projects in support of GE Plastics.

Today she is responsible for leading GE’s nano research programs, one of six advanced technology programs at GE Global Research. She is married and has two children ages 13 and 10.

August 31, 2007 – Algan KK, a spinoff from Japan’s Doshisha U. building devices with aluminum gallium nitride (AlGaN) semiconductor materials, says it has developed a highly-sensitive and tunable sensor for UV radiation that’s twice as reliable as a silicon-based device, with anticipated application in the semiconductor industry, reports the Nikkei Business Daily.

The new sensor can handle exposure to powerful UV radiation and can detect a broad range of wavelengths within the UV band. Silicon-based sensors have a limited range and begin to lose sensitivity after a month, but the AlGaN sensors can operate for two months with no performance deterioration, detecting UV wavelengths shorter than 200nm, the paper notes. The company also can adjust the materials ratio to make custom sensors for specific wavelengths, e.g. 360nm light.

The company plans to market the new sensors as early as this year as a device that can monitor wavelength and strength of UV light used in circuitry patterning, and shorter wavelength UV light used to wash chips, the paper notes. Pricing is to be set at ~10,000 yen (US ~$86), with projected sales of 100 million yen (about $865,000) in the next fiscal year.

August 31, 2007 — Micropelt GmbH, manufacturer of thin film thermoelectric devices, has announced a significant technology advancement in its ultra-small, microchip thermoelectric coolers (TECs). The new MPC-D303 Series, one of Micropelt’s smallest TECs with a cold side area of only 0.98 square millimeters (mm2), supports a maximum temperature difference (delta T) of more than 60 Kelvin (K). This increased delta T (from 40K) opens possibilities for laser and photonic sensor manufacturers whose applications require a large bandwidth of thermal control.

The Micropelt MPC-Dx series has cooling power up to 100watts/cm2 and can realize temperature changes faster than 180K/second. It is perfect for highly dynamic thermal control with 10K ramps in just a few milliseconds. Its high cooling power density optimally supports small devices’ high cooling requirements. Based on Micropelt’s exclusive thin film thermoelectric technology, the cooler’s core is sputtered material that can be structured to exactly match the thermal and electrical requirements of many applications. This match can reduce overall energy consumption and improve thermal management.

The MPC-D303 is fabricated on silicon wafer using standard semiconductor processes. The device soldering temperature is 300 degrees Celsius and uses lead-free solder. It has a maximum operating temperature of 200 degrees Celsius. This chip-sized thermoelectric cooler offers superior performance for chip scale thermal management and fast, precise temperature control. Perfectly adapted designs, from less than 1mm2 to 25mm2, each with customizable thermal and electrical properties including sensor integration, open new dimensions of thermal management.

Applications include laser and sensor temperature management, micro-scale thermal cycling, lab-on-a-chip, single well to large array PCR cycling, technical device characterization, and printed circuit board embedded device cooling.

“Ever increasing integration and packaging densities are driving photonics development to smaller, faster, better performing products,” said Dr. Joachim Nurnus, CTO of Micropelt. “Our advanced thin film thermoelectric platform technology holds exciting potential for further cooler miniaturization in the photonics, microelectronics, and life science worlds.”

Volume prices for Micropelt MPC-D303 thermoelectric coolers will be below $10.

August 28, 2007 – Edwards (nee BOC Edwards, renamed this summer to reflect new private-equity ownership) has sold “the majority” of its “Kachina” semiconductor equipment parts cleaning/refurbishment business to Applied Materials for an undisclosed sum, and its stake in another part of the business in Taiwan, in order to focus on “profitable growth” in its core vacuum and abatement areas.

Under terms of the deals, Applied will purchase operations at facilities in Austin, TX; Phoenix, AZ; and Hillsboro, OR, as well as on-site operations at customer sites in Israel, Ireland, and Virginia. The assets will be folded into Applied’s global services arm, which already owns/operates parts cleaning service facilities in North America, Europe, Israel, Taiwan, Singapore, and China. BOC Edwards will retain the division’s operations in France and the UK.

“Kachina has more than 15 years of experience and knowledge in parts cleaning and coating and has an excellent reputation with its customers for delivering quality products,” said Mark Stark, GM of Applied’s fab operation services division, in a statement. “Building on our extensive global infrastructure, this strategic investment will add to Applied’s fab-wide service offerings and increase our capacity to deliver world-class chamber performance management to customers internationally.”

In a separate transaction, Edwards said it has sold its shareholding interest in BOC Edwards HTC Ltd., a parts cleaning services provider in Taiwan, to that business’s other shareholder, Highlight Tech Corp.

“The sale of the Kachina parts cleaning business to Applied Materials will enable Edwards to focus resources on providing world leading products and services either side of the process tool and on the profitable growth of its core vacuum and abatement business,” stated Nigel Hunton, CEO of Edwards.

In addition to front-end materials such as polishing pads, slurries, and pad conditioners for CMP, Rohm and Haas supplies SMIC with electroplating processes for wafer bumping and under bump metallization, photoresists and anti-reflectants used in lithography, and ion exchange resins used to produce ultrapure water needed in semiconductor manufacturing.

(August 29, 2007) DURHAM, NC &#151 In a move to reduce form factor while increasing power of its UHF power amplifiers, MILMEGA Ltd. has chosen Cree silicon carbide (SiC) MESFETS to power its new line. Cree’s SiC MESFETs are said to provide greater power density than conventional semiconductor materials, allowing for improved efficiency and more capabilities in a smaller form factor.

August 28, 2007 — GE Inspection Technologies has signed a definitive agreement to acquire phoenix|x-ray, developer of high-resolution computed tomography (CT) / X-ray technology used in non-destructive testing (NDT) applications.

The acquisition broadens GE’s NDT offerings, adding 3D computed tomography, micro- and nanotechnology systems to the company’s portfolio. This expanded technology suite will serve a wide variety of GE’s customers in the aerospace, power generation, oil & gas, automotive, industrial, and microelectronics industries.

“Phoenix|x-ray has a strong reputation in the non-destructive testing world and is a highly complementary addition to GE Inspection Technologies’ X-ray product line,” said Caroline Reda, President & CEO of GE Inspection Technologies. “The acquisition will enhance GE’s technology in X-ray testing machines, adding CT capability that has a much finer resolution than our current GE technology. This resolution capability for metal and composite imaging is integral to our mission to provide customers with a broad portfolio of high-tech and valuable non-destructive testing solutions.”

Passing harsh environment tests, highly accelerated stress tests (HAST), and other qualifiers brings MEMS-based timing viability for high-volume manufacturing, said Ed Grant, VP North American products and operations, Vectron International, a strategic partner of Discera. High-temperature storage test, thermal shock tests, and others are typical for quartz-based devices, added Bahle, noting that HAST and further, more rigorous tests were borrowed from semiconductor qualification environments.

(August 28, 2007) PHEONIX, AZ &#151 Semiconductor Manufacturing International Corporation honored Rohm and Haas Electronic Materials, CMP Technologies with the company’s 2007 Excellent Supplier Award, recognizing the efforts of the four Rohm and Haas business units that support SMIC: CMP Technologies, Microelectronic Technologies, Packaging and Finishing Technologies and Ion Exchange Resins. The criteria evaluated in choosing award recipients included quality, cost, on-time delivery, service and the environment.

August 27, 2007 – Nanometrics says it has completed the sale of facilities in Narita, Japan, related to the flat-panel display business that it sold in 2005 and “had sat unutilized” ever since. Also sold was a residential condo near the company’s headquarters in Milpitas, CA. Together the sales will add about $2 million in cash and both reduce debt and add income of approximately $1.2 million in 3Q07.

Tim Stultz, the newly appointed president/CEO of Nanometrics, pointed out the asset sales represent another example of the company monetizing fixed assets and getting rid of noncritical businesses, citing the recent sale of its machining and plating shop.

In the past year the company has also sold off its Yosemite CD-SEM and DiVA product lines, consolidated its overlay metrology production in Korea, and seen former CEO John Heaton and CFO Dave McCutcheon leave the company.

The character of RF design has changed quite dramatically in the past few years. It’s quite rare that RF designs are isolated pieces of circuitry, but rather part of a much bigger context. While the classic RF design is seen as a self-contained, small RF module, today’s RF designs typically are much larger and much more complex. Above all, they are multi-technology designs consisting of multiple RF modules integrated with high-speed digital, analog, power, and bias networks, all in close proximity on the same dense circuit board.

(August 27, 2007) SAN JOSE, CA &#151 Discera, Inc., qualified its MEMS-based oscillators with a series of frequency-stability and standard semiconductor qualification and reliability tests, comparing the silicon-based MEMS resonators to quartz for timing devices. Discera tested three separate manufacturing lots to prove process consistency in high-volume production, said Venkat Bahle, VP of marketing, Discera.